A further embodiment of the invention includes a method for stabilizing a hydroquinone composition (with about 1% to about 12% hydroquinone, preferably about 2% to about 10%, more preferably about 2% to about 8%, and most preferably about 3% to about 4%) with a neutral pH of from about 5.5 to about 8.0, more preferably a pH of from about 5.5 to about 7.5, and most preferably at a pH of from about 6.0 to about 7.5, by adding a water-soluble antioxidant, preferably sulfite, including but not limited to sulfites, bisulfites, metabisulfites, their salts and their derivatives, most preferably sodium metabisulfite, and a cationic salt of acidic ascorbyl esters, preferably sodium ascorbyl phosphate, more preferably aminopropyl ascorbyl phosphate, most preferably magnesium ascorbyl phosphate. Get medical attention. Antioxidants in the hydroquinone phase are instrumental in stabilizing the color of the hydroquinone composition. Determination and Correlation of Solubilities of Benzoic Acid, Salicylic Acid, Resorcinol and Hydroquinone in Water and in 1-Octanol at Temperatures from 297.25K to 334.45K. ORIGINAL CODE: 0009013, Ref document number: Inhalation Remove to fresh air. [34], It is also one of the chemical compounds found in castoreum. Hydroquinone is considered to be readily biodegrable and photodegradable. 0.5% magnesium ascorbyl phosphate protected at pH 6.0-7.0, 1.0-1.5% at pH 5.5-7.0, and 2.0-3.0% at pH 3.5-7.0. Provided by the Springer Nature SharedIt content-sharing initiative, Over 10 million scientific documents at your fingertips, Not logged in Eng. N')].uJr These can be burning, redness, sensitization and irritation in some patients. Methylaminophenol, used in photography, is produced in this way:[8]. 2 Liquid phase only; silicon dioxide remains as a residue in these solvents. Phase A: Dissolve L-Ascorbic Acid in distilled water via agitation and gentle heating (warm, never hot or you will denature the ascorbic acid). 0000002585 00000 n 109. 2005 Wiley-VCH, Weinheim. Unfortunately, retinoids, in particular retinoic acid, retinal, and their derivatives, isomers and analogs (such as adapalene, tazarotene and isotretoin) also have discoloration problems due to oxidation. In the environment, hydroquinone showed increased toxicity for aquatic organisms, being less harmful for bacteria and fungi. It is a reducmg agent that is reversibly oxidized to semiquinone and quinone. Get medical attention. protecting the retinoids in a protective system; mixing the hydroquinone, and the protected retinoids; and. V)gB0iW8#8w8_QQj@&A)/g>'K t;\ $FZUn(4T%)0C&Zi8bxEB;PAom?W= fungichromin, Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. Hydroquinone compositions are effective but have some undesirable side effects. Hydroquinone is a white, odorless, crystalline solid with an extremely low vapor pressure. ChemPoint will not under any circumstances release personal user information to individuals or companies. HYdroquinone can be found in various skin care products. 0000008514 00000 n SAS Anti-ox booster 1% 0.3g. Formula of hydroquinone is . Conversion factors (at 25C and normal atmospheric pressure) 1 ppm = 4.5 mg/m 3 1 mg/m 3 = 0.222 ppm Table 1. endstream endobj 382 0 obj << /Type /FontDescriptor /Ascent 891 /CapHeight 656 /Descent -216 /Flags 34 /FontBBox [ -558 -307 2034 1026 ] /FontName /BCGJCE+TimesNewRoman,Bold /ItalicAngle 0 /StemV 160 /XHeight 0 /FontFile2 389 0 R >> endobj 383 0 obj << /Type /Font /Subtype /TrueType /FirstChar 32 /LastChar 181 /Widths [ 250 0 0 0 0 0 0 278 333 333 500 0 250 333 250 278 500 500 500 500 500 500 500 500 500 500 333 333 0 570 0 0 0 722 667 722 722 667 611 778 778 389 500 778 667 944 722 778 611 778 722 556 667 722 722 1000 722 722 0 333 0 333 0 0 0 500 556 444 556 444 333 500 556 278 333 556 278 833 556 500 556 556 444 389 333 556 500 722 500 500 444 0 0 0 0 0 0 0 0 0 0 0 500 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 500 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 576 ] /Encoding /WinAnsiEncoding /BaseFont /BCGJCE+TimesNewRoman,Bold /FontDescriptor 382 0 R >> endobj 384 0 obj << /Type /FontDescriptor /Ascent 929 /CapHeight 0 /Descent -249 /Flags 32 /FontBBox [ -184 -249 1037 929 ] /FontName /BCGKAB+ImprintMT-Shadow /ItalicAngle 0 /StemV 0 /FontFile2 390 0 R >> endobj 385 0 obj << /Type /Font /Subtype /TrueType /FirstChar 32 /LastChar 122 /Widths [ 250 0 0 0 0 0 0 0 323 323 0 0 0 375 240 0 510 427 510 510 0 510 0 510 510 510 0 0 0 0 0 0 0 729 0 729 0 698 0 0 854 0 0 0 0 927 802 813 0 0 0 604 0 0 0 0 802 0 0 0 0 0 0 0 0 448 552 0 552 448 0 0 573 271 0 0 271 875 573 500 0 552 375 0 323 573 0 0 0 500 448 ] /Encoding /WinAnsiEncoding /BaseFont /BCGKAB+ImprintMT-Shadow /FontDescriptor 384 0 R >> endobj 386 0 obj << /N 3 /Alternate /DeviceRGB /Length 2575 /Filter /FlateDecode >> stream Then take the water and put the measurement into the microwave until boiled. Hydroquinone IS a white crystalline substance when pure and is highly soluble in water. Table I shows that at 5C, 4% hydroquinone compositions maintain their white color with the addition of at least about 0.01% sodium metabisulfite at the low pH ranges (from about 3.50 to about 5.50) and at least 0.05% sodium metabisulfite for pH about 6.0 to about 7.0. Hydroquinone is 1,4-benzenediol. Johnson & Johnson Consumer Products, Inc. Johnson & Johnson Consumer Companies, Inc. AT BE CH CY DE DK ES FI FR GB GR IE IT LI LU MC NL PT SE TR, STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN, Color Stability of 4% HQ Compositions with varying pH and % Sodium Metabisulfite at 5C and 40C, Color Stability of 4% HQ Compositions with varying pH and % Magnesium Ascorbyl Phosphate at 5C and 40C, Polyacrylamide (and) C 13-14 isoparaffin (and) laureth-7, Water, Soybean (Glycine Soja) Oil, Carnauba (Copemicia Cerifera), wax, tocopherol, retinol, Ceteareth-20, Water, Soybean (Glycine Soja) Oil, Carnauba (Copernicia Cerifera), wax, tocopherol, retinol, Ceteareth-20, Compositions for the treatment of pigmentation disorders and methods for their manufacture, Stabilization composition including hydroquinone or derivative thereof, Stabilized retinol for cosmetic dermatological, and pharmaceutical compositions, and use thereof, Depigmenting composition for the skin comprising adapalene and at least one depigmenting agent, Depigmenting composition for the skin, use of a depigmenting composition for the skin, cosmetic use of the same and method for non-therapeutic cosmetic treatment, Cosmetic designs and products using intronic RNA, Holistic composition and method for reducing skin pigmentation, Topical compositions and methods of manufacturing them in specifically treated steel vessels, System for improved percutaneous absorption of skin benefiting agents, Discontinuous surface coating for particles, Method of treating skin requiring chemical peel procedure, Method of treating skin needing hyaluronic acid treatment, Method of treating skin having incision from surgical procedures, Method of treating skin requiring hair removal procedure, Method of treating skin requiring Intense Pulse Light (IPL) procedure, Method of treating skin subject to or affected by aesthetic surgical procedures, Method of treating skin needing ablative treatment, Method of treating skin requiring radiofrequency procedure, Method of treating skin requiring non-ablative procedure, Method of treating skin requiring fractional resurfacing treatment, Method of treating skin needing botulinum toxin type a treatment, Method of treating skin requiring microdermabrasion, Method of treating skin needing collagen treatment, Method of treating skin requiring skin cancer treatment, Methods of treating skin to enhance therapeutic treatment thereof, Ras mutation and compositions and methods related thereto, Compositions, kits and regimens for the treatment of skin, especially dcolletage, Calcium sequestration compositions and methods of treating skin pigmentation disorders and conditions. We will respond to you shortly. HYPERPIGMENTARY STAIN ELIMINATING CREAM FOR FACE SKIN AND ITS USE. Solubility of Hydroquinone in Different Solvents from 276.65 K to 345. Have an order or account question? 0000085850 00000 n In hydroquinone and sodium metabisulfite compositions, it is believed that the sodium metabisulfite oxidizes first and delays the start of any oxidation of the hydroquinone, so that excessive discoloration is delayed or totally avoided. Reference Tables: SOLUBILITIES - uspbpep.com Ferulic acid 0.5% 0.15g. Thank you for your inquiry and interest in ChemPoint. When the contents of the reservoir are forced into the reaction chamber, the catalases and peroxidases rapidly break down the hydrogen peroxide and catalyze the oxidation of the hydroquinones into p-quinones. Calorim. C6H4O2) is formed. Solubility of Hydroquinone. 0000053439 00000 n trailer << /Size 393 /Info 347 0 R /Root 375 0 R /Prev 573815 /ID[<6893db2526a970a0c364cca2e99ca522>] >> startxref 0 %%EOF 375 0 obj << /Type /Catalog /Pages 346 0 R /Metadata 348 0 R >> endobj 391 0 obj << /S 2217 /Filter /FlateDecode /Length 392 0 R >> stream Hydroquinone occurs in the environment as a result of anthropogenic processes, as well as in natural products from plants and animals. Hydroquinone is an aromatic organic compound which is currently used in two main sectors: . New experimental data are provided for the solubility of resorcinol in water and salicylic acid, resorcinol, hydroquinone in 1-octanol. Some products also contain sunscreens. 1401417, Country of ref document: Then take the water and put the measurement into the microwave until boiled. Glycerol derivatives solubilise natural, hydrophilic antioxidants in biofuels. Monobenzone: Uses, Interactions, Mechanism of Action - DrugBank This page was last modified on 19 June 2019, at 20:05. 250, 165172 (2006), F. L. Mota, A. J. Queimada, A. E. Andreatta, S. P. Pinho, E. A. Macedo, Fluid Phase Equilib. It is soluble in water. Hydroquinone is combustible when preheated. I did that by using 1 cup of cream, 4tbsp of hydroquinone and 4tbsp of water or solvent. 77, No. How do I dissolve hydroquinone powder to make a 20% and 10% concentration? Add the hydroquinone to the water. Chem. 57, 295300 (2013), R. F. Pires, M. R. Franco Jr, Fluid Phase Equilib. Free format text: Eastman Hydroquinone, USP Grade is for skin-lightening products to address hyperpigmentation. 2y.-;!KZ ^i"L0- @8(r;q7Ly&Qq4j|9 For a shipping quote, check the box and the bottom and provide us your shipping information. Skin Contact Wash off immediately with plenty of water for at least 15 minutes. 552591, Z. Esina, M. Korchuganova, Theor. Data 51, 16681671 (2006), C. L. Yaws, S.-C. Lin, Enthalpy of fusion at freezing pointOrganic compounds, in Thermophysical Properties of Chemicals and Hydrocarbons, William Andrew Publishing (Elsevier, 2009), pp. Chem. 2017-02-16T10:10:56+01:00 Boucif Belhachemi. Re: How to dissolve Hydroquinone to make 4 oz. Protected retinoid, with its skin benefit capabilities, may also be included with the hydroquinone composition. Conversion factors (at 25 oc and normal atmospheric pressure) 1 ppm = 4.5 mg!m 3 Eng. It would be desirable to combine the pigmentation disorder treatment with this skin benefit ingredient in one composition. Therefore, the solubility values of hydroquinone in different solvents are required; however, the data availability in the literature is poor.3-7 In this work, the solubility data of hydroquinone in water, methanol, ethanol, 2-propanol, ethyl acetate, butyl acetate, and acetic acid from 276.65 K to 345.10 K under atmospheric pressure were . These phases (described below) are combined in a mixing tank with an in-line homogenizer as follows. This compound is gathered from the beaver's castor sacs.[35]. 338, 217223 (2013), S. H. Ali, F. S. Al-Mutairi, M. A. Fahim, Fluid Phase Equilib. It can also be found on eBay and Amazon. However, hydroquinone discolors at the pH range of 7.0 to 8.5. Hydroquinone is combustible when preheated. A3, Free format text: The obtained results show that the . Eng. Then add it to the ingredients. [O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(O)=C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1, OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C, Antibiotics FOR TREATMENT OF HEMORRHOIDS AND ANAL FISSURES FOR TOPICAL USE, CCCCCCCCCCCCCCCC(=O)OC[C@H](O)[C@H]1OC(=O)C(O)=C1O, [(2R)-2-[(1S)-1,2-dihydroxyethyl]-3-hydroxy-5-oxo-2H-furan-4-yl] dihydrogen phosphate, [Na+]. Using a laser-monitoring observation technique, the solubility of hydroquinone in water, methanol, ethanol, 2-propanol, ethyl acetate, butyl acetate, and acetic acid were measured at temperatures ranging from 276.65 K to 345.10 K under the atmospheric pressure. Remove contact lenses, if present and easy to do. 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Examples of suitable methods of encapsulation include encapsulation by liposomes, wax, paraffin or any material or combination of materials which protect the retinoid from exposure to oxygen and inhibit oxidation of the retinoid from oxidation. Thanks to the added vitamin E, it leaves your skin feeling smooth and soft, too. J. Chem. I understand the concentrations are high but I have used them before, its just too expensive to keep buying from a compounding pharmacy. 0000002379 00000 n HYDROQUINONE (DIHYDROXYBENZENE) | Occupational Safety and Health Find answers in our support articles. I can only tell you how to mix the powder solution to the liquid solvent. Classical photo shops also sell hydroquinone. RJPT - Hydroquinone Solubility in Pure and Binary Solvent Mixture at The Density of hydroquinone is . [31], Hydroquinones are one of the two primary reagents in the defensive glands of bombardier beetles, along with hydrogen peroxide (and perhaps other compounds, depending on the species), which collect in a reservoir. Phase B: Dissolve the ferulic acid in the glycerin - some "spirited" stirring may be necessary. One embodiment of the invention is a composition which comprises hydroquinone (about 1% to about 12%, preferably about 2% to about 10%, more preferably about 2% to about 8%, more preferably with about 2% to about 4%, and most preferably about 3% to about 4%) and has a neutral pH of from about 5.5 to about 8.0, more preferably a pH of from about 5.5 to about 7.5, and most preferably at a pH of from about 6.0 to about 7.5. So, does anybody know of another solvent I could use that has a higher . The solubility in water is 6.72g/L. Mobility in soil No additional information available 12.5. Some documentation and label information may refer to the legacy brand. INCI HydroquinoneEastman Hydroquinone, USP is a skin care ingredient used to produce effective skin- lightening applications for depigmentation. Airborne hydroquinone may be oxidized to quinone at ordinary . The solubilities of benzoic acid, salicylic acid, resorcinol and hydroquinone in water and in 1-octanol were measured by the dynamic method which is also called the synthetic method from 297.25 K to 334.45 K. Using differential scanning calorimetry (DSC Q2000 and SDT Q600), the melting temperature and the enthalpy of fusion of these solutes were determined. The FDA had classified hydroquinone in 1982 as a safe product - generally recognized as safe and effective (GRASE), however additional studies under the National Toxicology Program (NTP) were suggested in order to determine whether there is a risk to humans from the use of hydroquinone. Protected retinoid may be added to these compositions for additional skin benefit effects. This saturated dicarboxylic acid exists as a white powder. The experimental solubilities were correlated using two regression equations. Do not put this product in the microwave. endstream endobj 1 0 obj <> endobj 2 0 obj <> endobj 12 0 obj <>stream It has a white-solid appearance. If you are already a ChemPoint customer then sign up for access to our online ordering website. Other antioxidants, for example cationic salts of acidic ascorbyl esters, most preferably magnesium ascorbyl phosphate, aminopropyl ascorbyl phosphate, and sodium ascorbyl phosphate, have not been utilized in combination with hydroquinone in view of the acidic pH, generally from about 3.4 to about 3.5, and the recommended pH range for magnesium ascorbyl phosphate is about 7.0 to 8.5. Classical photo shops . Hydroquinone | C6H4(OH)2 or C6H6O2 | CID 785 - structure, chemical names, physical and chemical properties, classification, patents, literature, biological activities . Pigmentation disorders can take a variety of forms like hyperpigmentation and hypopigmentation, such as melasma (dark patches experienced in pregnancy), liver spots (which often develop with age), as a side effect of birth control pills, and as a persistent result of acne, bums, bites and other skin injuries, and vitiligo. I'd like the consistency to be thin like a gel so that it absorbs quicker. Discoloration of hydroquinone compositions may be accelerated by repeated exposure to oxygen or exposing the compositions to high temperatures, which may be found inside a car or delivery vehicle on a hot sunny day. S.C. Gad, T. Pham, in Encyclopedia of Toxicology (Third Edition), 2014 Environmental Fate and Behavior. Data 53, 12781282 (2008), A. Hydroquinone is a white crystalline solid, poorly soluble in water, but more soluble in organic solvents. uv curable cellulose estersuv curable cellulose esters . . Bioaccumulative potential Hydroquinone (123 -31 -9) Bioaccumulative potential Not established. Thus, while cationic salts of acidic ascorbyl esters, preferably magnesium ascorbyl phosphate and aminopropyl ascorbyl phosphate, have beneficial antioxidant effects on the skin, the combination with hydroquinone in the invention results in a compatible and stable composition. ADS . [17], An important reaction is the conversion of hydroquinone to the mono- and diamine derivatives. Hydroquinone[1] Idrochinone Quinol 1,4-Dihydroxybenzene p-dihydroxybenzene p-hydroxyphenol 1,4-Hydroxy benzene Identifiers CAS Number 123-31-9 Y 3D model (JSmol) Interactive image Beilstein Reference 605970 ChEBI CHEBI:17594 Y ChEMBL ChEMBL537 Y ChemSpider 764 Y DrugBank DB09526 ECHA InfoCard 100.004.199 EC Number 204-617-8 Gmelin Reference 2742 Hydroquinone - Sciencemadness Wiki AzA inhibits tyrosinase. Hydroquinone, like phenols are very weak acids and can be deprotonated. Hydroquinone composition - SCHERING CORP - FreePatentsOnline.com The color stability of the hydroquinone composition is promoted by one or more antioxidants in the hydroquinone phase, preferably sulfite, including but not limited to sulfites, bisulfites, metabisulfites, their salts and their derivatives, most preferably sodium metabisulfite, and a cationic salt of acidic ascorbyl esters, most preferably magnesium ascorbyl phosphate. Hydroquinone is a white crystalline solid, poorly soluble in water, but more soluble in organic solvents. Hydroquinone - an overview | ScienceDirect Topics Editor's Rating: We have discovered that a hydroquinone composition (with about 1 to about 12% hydroquinone, preferably with about 2% to about 10%, more preferably with about 2% to about 8%, more preferably with about 2% to about 4%, most preferably with about 3% to about 4% hydroquinone) with preferably a pH of from about 5.5 to about 8.0, more preferably a pH of from about 5.5 to about 7.5, and most preferably at a pH of from about 6.0 to about 7.5, can include cationic salts of acidic ascorbyl esters, preferably sodium ascorbyl phosphate, more preferably aminopropyl ascorbyl phosphate, most preferably magnesium ascorbyl phosphate as an antioxidant and the color destabilization problems are appreciably less as compared to hydroquinone compositions without such a cationic salt of acidic ascorbyl esters in the neutral pH range: preferably a pH of from about 5.5 to about 8.0, more preferably a pH of from about 5.5 to about 7.5, and most preferably at a pH of from about 6.0 to about 7.5. Eye Contact Rinse immediately with plenty of water, also under the eyelids, for at least 15 minutes. This website uses cookies. The protective system can be an entrapment system, a single or multi- laminar system, such as by the formation of vesicles such as a liposome or by utilizing wax, paraffin, silicone, polyethylene, or any material or system which protects the retinoid from oxidation. Have an order or account question, find answers in our Online Support articles. Eastman Hydroquinone, USP, meets or exceeds the requirements of the United States Pharmacopoeia and is produced under conditions of current good manufacturing practices (cGMP). This is seen at about a pH of 3.50 with at least about 2.0% magnesium ascorbyl phosphate, and again at a pH of about 6.5 to about 7.0 with at least about 2.0% magnesium ascorbyl phosphate. Such carriers are widely known in the art and deliver the composition's ingredients to the skin without excessive degradation, inactivation or other unwanted interaction. Hydroquinone skin cream, gel, emulsion, lotion, or solution Hydroquinone Safety Data Sheet according to Federal Register / Vol. We apologize! Variations in pH have proven to result in excessive discoloration ranging from brownish to black. At 40C, 4% hydroquinone compositions have the same color stability with slightly more sodium metabisulfite, at least about 0.01% at about 3.5 to about 4.0 pH; at least about 0.05% sodium metabisulfite at about 4.5 to about 6.0 pH; and at pH; at least about 0.05% sodium metabisulfite at about 4.5 to about 6.0 pH; and at least about 0.10% sodium metabisulfite at about 6.5 to about 7.0 pH. Gerhard Franz, Roger A. Sheldon "Oxidation" in. The disodium diphenolate salt of hydroquinone is used as an alternating comonomer unit in the production of the polymer PEEK. Continue rinsing.IF SWALLOWED: Call a POISON CENTER or doctor/physician if you feel unwell.Avoid release to the environment.WARNING: The information provided on this web site was developed in compliance with European Union (EU) regulations and is correct to the best of our knowledge, information and belief at the date of its publication. PDF HYDROQUINONE HEALTH AND SAFETY GUIDE - World Health Organization The experimental solubility data was well-correlated with the data, calculated by . Hydroquinone (EHC 157, 1994) - International Programme on Chemical Safety
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